Iranian Journal of Materials Science and Engineering
Iran University of Science & Technology
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Volume 8, Issue 3 (september 2011 2011)
IJMSE 2011, 8(3): 29-36 |
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A. Namiranian, M. Kalantar. MULLITE SYNTHESIS AND FORMATION FROM KYANITE CONCENTRATES IN DIFFERENT CONDITIONS OF HEAT TREATMENT AND PARTICLE SIZE. IJMSE 2011; 8 (3) :29-36
URL: http://ijmse.iust.ac.ir/article-1-379-en.html
URL: http://ijmse.iust.ac.ir/article-1-379-en.html
Abstract: (31536 Views)
The process of mullitization of kyanite concentrate was studied at different conditions of heat treatment (1400
– 1600 °C and 0.5 – 3.5 hours) and particle size of raw materials (38-300 ?m). Kyanite concentrate was obtained from
ore-dressing of kyanite deposits of Mishidowan-Bafgh region at 100 km northeastern part of Yazd. The results of
microstructure (shape, distribution and size of the grains) and phase evolution studies by SEM and XRD showed that
total transformation of kyanite to mullite takes place by heat treatment between 1500 –1550 °C during 2.5 hours.. At
temperatures below 1500 °C need-like mullite grains are always produced. At higher temperatures the mullite grains
reveal rounded and platelet morphology. At 1550 °C, the rate of mullitization and densification were improved by
increasing soaking time from 1h to 3h and decreasing particle size of materials from 300 to 38 m
– 1600 °C and 0.5 – 3.5 hours) and particle size of raw materials (38-300 ?m). Kyanite concentrate was obtained from
ore-dressing of kyanite deposits of Mishidowan-Bafgh region at 100 km northeastern part of Yazd. The results of
microstructure (shape, distribution and size of the grains) and phase evolution studies by SEM and XRD showed that
total transformation of kyanite to mullite takes place by heat treatment between 1500 –1550 °C during 2.5 hours.. At
temperatures below 1500 °C need-like mullite grains are always produced. At higher temperatures the mullite grains
reveal rounded and platelet morphology. At 1550 °C, the rate of mullitization and densification were improved by
increasing soaking time from 1h to 3h and decreasing particle size of materials from 300 to 38 m
Keywords: Kyanite, Kinetic of mullitization, Heat treatments, Densification, Microstructure, Mishidowan-Bafgh deposits
Type of Study: Research Paper |
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