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Highlights
• Ni-Co/SiC-CeO2 composite coating was prepared on a copper substrate using the pulse electrodeposition method.
• Higher current densities (0.1, 0.2, 0.3 A/cm²) lead to an increase in microhardness as a result of grain refinement.
• Increasing the duty cycles (10, 20, 30 %) leads to a decrease in microhardness due to lower nanoparticle concentration.
• Higher duty cycles result in a reduction in corrosion resistance, as they mimic a DC state.
• Higher frequencies (10, 100, 1000 Hz) improve both microhardness and corrosion resistance.